By Robert A. Stockland
A pragmatic guide for chemists acting bond forming reactions, this publication beneficial properties worthwhile details at the synthesis of universal useful teams in natural chemistry.
- information smooth practical team synthesis via carbon-heteroelement (N, O, P, S, B, halogen) bond forming reactions with a spotlight on operational simplicity and sustainability. - Summarizes key and up to date advancements - that are differently scattered throughout magazine literature - right into a unmarried resource- includes over a hundred targeted arrangements of universal useful teams- incorporated 25 troubleshooting courses with feedback and strength suggestions to universal problems.- enhances the textual content in superior e-book variations with educational video clips the place the writer presents an creation to microwave assisted chemistry.
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A realistic instruction manual for chemists acting bond forming reactions, this booklet gains precious info at the synthesis of universal useful teams in natural chemistry.
- information smooth sensible staff synthesis via carbon-heteroelement (N, O, P, S, B, halogen) bond forming reactions with a spotlight on operational simplicity and sustainability. - Summarizes key and up to date advancements - that are another way scattered throughout magazine literature - right into a unmarried resource- includes over a hundred particular arrangements of universal practical teams- integrated 25 troubleshooting courses with feedback and power suggestions to universal difficulties. - enhances the textual content in greater book variants with educational video clips the place the writer presents an advent to microwave assisted chemistry.
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Extra info for Practical Functional Group Synthesis
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J. Am. Chem. Soc. 1994, 116, 3684–3691. ; Wang, Z. Angew. Chem. Int. Ed. 2012, 51, 8077–8081. 1 PREPARATION OF ALCOHOLS, ETHERS, AND RELATED COMPOUNDS THROUGH THE FORMATION OF OXYGEN–CARBON(sp3) BONDS Alcohols are arguably the simplest and most common oxygen‐containing functional groups. For secondary and tertiary alcohols, one of the most popular synthetic approaches entails the addition of Grignard and organolithium reagents to carbonyl‐containing compounds. For these reactions, the oxygen is already attached to the framework.
Determining how much power is needed can often be the critical aspect of the synthetic design. The good news is that due to the operational simplicity of modern microwave reactors, finding a good set of conditions often takes less than a day. For high‐absorbing materials such as DMF or ionic liquids, this power level could be quite low. Once the minimum power level has been determined, increasing/decreasing the power setting for subsequent screening reactions in 10–20% increments and analyzing the results will rapidly provide an experimental determination of how much microwave power is needed to achieve a desired result.