Download Analytical Chemistry of the Actinide Elements by Alfred J. Moses PDF

Download Analytical Chemistry of the Actinide Elements by Alfred J. Moses PDF

By Alfred J. Moses

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W I S H , Anal. , 3 1 , 326 (1959). 330 (1959). 14. G . R . C H O P P I N , J. Chem. , 36, 462 (1959). 15. G . R . C H O P P I N a n d R . J . SILVA, J. Inorg. and Nuclear (1956). 16. , 3 , 153 S . G . T H O M P S O N , Β . G . H A R V E Y , G . R . C H O P P I N a n d G . T . SEABORG, J. Am. Chem. Soc, 76, 6229 (1954). 17. S . G . T H O M P S O N , U . S . A t o m i c E n e r g y C o m m . R e p . U C R L - 8 6 1 5 , 1959. 36 THE ACTINIDE ELEMENTS 18. G. R. CHOPPIN, B. F . HARVEY and S. G. THOMPSON, J.

42 paper. ) and 3 ml of potassium iodate solution (15 g of KIO3, dissolved in 100 ml of 1:1 HNO3 and filtered). Place the beaker containing the solution in cold H 2 0 overnight to obtain complete precipitation of thorium iodate. Filter the solution through Whatman No. ) and wash precipitate 4 times with wash solution. Transfer the precipitate into a beaker using H 2 0 to aid in the transfer. Wash the paper with a mixture of HC1 and H 2 S 0 3 and transfer wash into beaker containing the precipitate.

The method is applicable to the determination of uranium in the presence of thorium and potassium. N E U T R O N A C T I V A T I O N ANALYSIS Activation analysis involves the determination of the concentration of an element by measuring the radioactivity, induced by irradiation with nuclear radiation. The resultant radioisotopes are characterized by their half-lives, types and energies of emitted radiation, and their chemical behavior. The induced activity is proportional to the irradiation dose and the amount of element in the sample.

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